Carbon 13 NMR for common organic solvents.

  carbon THF-d8 CD2Cl2 CDCl3 toluene-d8 C6D6 C6D5Cl (CD3)2CO (CD3)2SO CD3CN TFE-d3 CD3OD D2O
solvent signals 67.21 53.84 77.16 137.48 128.06 134.19 29.84 39.52 1.32 61.5 49
    25.31     128.87   129.26 206.26   118.26 126.28    
127.96 128.25
          125.13   125.96            
20.43
acetic acid CO 171.69 175.85 175.99 175.3 175.82 175.67 172.31 171.93 173.21 177.96 175.11 177.21
CH3 20.13 20.91 20.81 20.27 20.37 20.4 20.51 20.95 20.73 20.91 20.56 21.03
acetone CO 204.19 206.78 207.07 204 204.43 204.83 205.87 206.31 207.43 32.35 209.67 215.94
CH3 30.17 31 30.92 30.03 30.14 30.12 30.6 30.56 30.91 214.98 30.67 30.89
acetonitrile CN 116.79 116.92 116.43 115.76 116.02 115.93 117.6 117.91 118.26 118.95 118.06 119.68
CH3 0.45 2.03 1.89 0.03 0.2 0.63 1.12 1.03 1.79 1 0.85 1.47
benzene CH 128.84 128.68 128.37 128.57 128.62 128.38 129.15 128.3 129.32 129.84 129.34  
tert-butyl alcohol (CH3)3C 67.5 69.11 69.15 68.12 68.19 68.19 68.13 66.88 68.74 72.35 69.4 70.36
  (CH3)3C 30.57 31.46 31.25 30.49 30.47 31.13 30.72 30.38 30.68 31.07 30.91 30.29
carbon dioxide CO2 125.69 125.26 124.99 124.86 124.76 126.08 125.81 124.21 125.89 126.92 126.31
carbon disulfide CS2 193.37 192.95 192.83 192.71 192.69 192.49 193.58 192.63 193.6 196.26 193.82 197.25
carbon tetracholoride CCl4 96.89 96.52 96.34 96.57 96.44 96.38 96.65 95.44 96.68 97.74 97.21 96.73
chloroform CH 79.24 77.99 77.36 77.89 77.79 77.67 79.19 79.16 79.17 78.83 79.44  
18-crown-6 CH2 71.34 70.47 70.55 70.86 70.59 70.55 71.25 69.85 71.22 70.8 71.47 70.14
cyclohexane CH2 27.58 27.38 26.94 27.31 27.23 26.99 27.51 26.33 27.63 28.34 27.96  
1,2-dichloroethane CH2 44.64 44.35 43.5 43.4 43.59 43.6 45.25 45.02 45.54 45.28 45.11
dichloromethane CH2 54.67 54.24 53.52 53.47 53.46 53.54 54.95 54.84 55.32 54.46 54.78  
diethyl ether CH3 15.49 15.44 15.2 15.47 15.46 15.35 15.78 15.12 15.63 15.33 15.46 14.77
  CH2 66.14 66.11 65.91 65.94 65.94 65.79 66.12 62.05 66.32 67.55 66.88 66.42
diglyme CH3 58.72 58.95 59.01 58.62 58.66 58.42 58.77 57.98 58.9 59.4 59.06 58.67
  CH2 71.17 70.7 70.51 70.92 70.87 70.56 71.03 69.54 70.99 73.05 71.33 70.05
CH2 72.72 72.25 71.9 72.39 72.35 72.07 72.63 71.25 72.63 71.33 72.92 71.63
dimethylformamide CH 161.96 162.57 162.62 161.93 162.13 162.01 162.79 162.29 163.31 166.01 164.73 165.53
CH3 35.65 36.56 36.5 35.22 35.25 35.45 36.15 35.73 36.57 37.76 36.89 37.54
  CH3 30.7 31.39 31.45 30.64 30.72 30.71 31.03 30.73 31.32 30.96 31.61 32.03
1,4-dioxane CH2 67.65 67.47 67.14 67.17 67.16 66.95 67.6 66.36 67.72 68.52 68.11 67.19
DME CH3 58.72 59.02 59.08 58.63 58.68 58.31 58.45 58.03 58.89 59.52 59.06 58.67
CH2 72.58 72.24 71.84 72.25 72.21 71.81 72.47 71.17 72.47 72.87 72.72 71.49
ethane CH3 6.79 6.91 6.89 6.94 6.96 6.91 6.88 6.61 6.99 7.01 6.98  
ethanol CH3 18.9 18.69 18.41 18.78 18.72 18.55 18.89 18.51 18.8 18.11 18.4 17.47
  CH2 57.6 58.57 58.28 57.81 57.86 57.63 57.72 56.07 57.96 59.68 58.26 58.05
ethyl acetate CH3CO 20.45 21.15 21.04 20.46 20.56 20.5 20.83 20.68 21.16 21.18 20.88 21.15
  CO 170.32 171.24 171.36 170.02 170.44 170.2 170.96 170.31 171.68 175.55 172.89 175.26
CH2 60.3 60.63 60.49 60.08 60.21 60.06 60.56 59.74 60.98 62.7 61.5 62.32
  CH3 14.37 14.37 14.19 14.23 14.19 14.07 14.5 14.4 14.54 14.36 14.49 13.92
ethylene CH2 123.09 123.2 123.13 122.92 122.96 122.95 123.47 123.52 123.69 124.08 123.46
ethylene glycol CH2 64.35 64.08 63.79 64.29 64.34 64.03 64.26 62.76 64.22 64.87 64.3 63.17
H grease CH2 30.45 30.14 29.71 30.31 30.22 30.11
hexamethylbenzene C 131.88 132.09 132.21 131.72 131.79 131.54 132.22 131.1 132.61 134.04 132.53  
CH3 16.71 16.93 16.98 16.84 16.95 16.68 16.86 16.6 16.94 17.04 16.9
n-hexane CH3 14.22 14.28 14.14 14.34 14.32 14.18 14.34 13.88 14.43 14.63 14.45  
CH2(2,5) 23.33 23.07 22.7 23.12 23.04 22.86 23.28 22.05 23.4 24.06 23.68
  CH2(3,4) 32.34 32.01 31.64 32.06 31.96 31.77 32.3 30.95 32.36 33.17 32.73  
HMDSO CH3 1.83 1.96 1.97 1.99 2.05 1.92 2.01 1.96 2.07 2.09 1.99 2.31
HMPA CH3 36.89 36.99 36.87 36.8 36.88 36.64 37.04 36.42 37.1 37.21 37 36.46
imidazole CH(2) 135.72 135.76 135.38 135.57 135.76 135.5 135.89 135.15 136.33 136.58 136.31 136.65
  CH(4,5) 122.2 122.16 122 122.13 122.16 121.96 122.31 121.55 122.78 122.93 122.6 122.43
methane CH4 -4.9 -4.33 -4.63 -4.34 -4.29 -4.33 -5.33 -4.01 -4.61 -5.88 -4.9
methanol CH3 49.64 50.45 50.41 49.9 49.97 49.66 49.77 48.59 49.9 50.67 49.86 49.5
nitromethane CH3 62.49 63.03 62.5 61.14 61.16 61.68 63.21 63.28 63.66 63.17 63.08 63.22
n-pentane CH3 14.18 14.24 14.08 14.27 14.25 14.1 14.29 13.28 14.37 14.54 14.39  
CH2(2,4) 23 22.77 22.38 22.79 22.72 22.54 22.98 21.7 23.08 23.75 23.38
  CH2(3) 34.87 34.57 34.16 34.54 34.45 34.26 34.83 33.48 34.89 35.76 35.3  
propane CH3 16.6 16.63 16.63 16.65 16.66 16.56 16.68 16.34 16.73 16.93 16.8
  CH2 16.82 16.63 16.37 16.63 16.6 16.48 16.78 15.67 16.91 17.46 17.19  
2-propanol CH3 25.7 25.43 25.14 25.24 25.18 25.14 25.67 25.43 25.55 25.21 25.27 24.38
  CH 66.14 64.67 64.5 64.12 64.23 64.18 63.85 64.92 64.3 66.69 64.71 64.88
propylene CH3 19.27 19.47 19.5 19.32 19.38 19.32 19.42 19.2 19.48 19.63 19.5
  CH2 115.74 115.7 115.74 115.89 115.92 115.86 116.03 116.07 116.12 116.38 116.04  
CH 134.02 134.21 133.91 133.61 133.69 133.57 134.34 133.55 134.78 136 134.61
pyridine CH(2,6) 150.57 150.27 149.9 150.25 150.27 149.93 150.67 149.58 150.76 149.76 150.07 149.18
CH(3,5) 124.08 124.06 123.75 123.46 123.58 123.49 124.57 123.84 127.76 126.27 125.53 125.12
  CH(4) 135.99 136.16 135.96 135.17 135.28 135.32 136.56 136.05 136.89 139.62 138.35 138.27
pyrrole CH(2,5) 118.03 117.93 117.77 117.61 117.78 117.65 117.98 117.32 118.47 119.61 118.28 119.06
  CH(3,4) 107.74 108.02 107.98 108.15 108.21 108.03 108.04 107.07 108.31 108.85 108.11 107.83
pyrrolidine CH2(2,5) 45.82 47.02 46.93 47.12 46.86 46.75 46.51 47.57 47.43 47.23 46.83
  CH2(3,4) 26.17 25.83 25.56 25.75 25.65   25.59 25.26 26.34 25.73 26.29 25.86
silicone grease CH3 1.2 1.22 1.19 1.37 1.38 1.09 1.4 2.87 2.1
tetrahydrofuran CH2(2,5) 68.03 68.16 67.97 67.75 67.8 67.64 68.07 67.03 68.33 69.53 68.83 68.68
CH2(3,4) 26.19 25.98 25.62 25.79 25.72 25.68 26.15 25.14 26.27 26.69 26.48 25.67
toluene CH3 21.29 21.53 21.46 21.37 21.1 21.23 21.46 20.99 21.5 21.62 21.5  
C(1) 138.24 138.36 137.89 137.84 137.91 137.65 138.48 137.35 138.9 139.92 138.85
  CH(2,6) 129.47 129.35 129.07 129.33 129.33 129.12 129.76 128.88 129.94 130.58 129.91  
CH(3,5) 128.71 128.54 128.26 128.51 128.56 128.31 129.03 128.18 129.23 129.79 129.2
  CH(4) 125.84 125.62 125.33 125.66 125.68 125.43 126.12 125.29 126.28 126.82 126.29  
triethylamine CH3 12.51 12.12 11.61 12.39 12.35 11.87 12.49 11.74 12.38 9.51 11.09 9.07
  CH2 47.18 46.75 46.25 46.82 46.77 46.36 47.07 45.74 47.1 48.45 46.96 47.19

Soure of data [1] Gottlieb, H. E.; Kotlyar, V.; Nudelman, A. J. Org. Chem. 1997, 62, 7512. [2] Fulmer, G. R. et al., Organometallics 2010, 29, 2176.